图3 NiO 的红外光谱图Fig.3 IR image of NiO 由图3 可知,衍射峰与标准卡片[JCPDS 卡30-0443]有很好的对应关系,产物为纯相Ni(OH)2[5],属于R3m(166)空间点阵群,其晶胞参数为a =0.296 221 nm,b =0.296 221 nm,c =0.725 008 nm(NiO 的标准晶胞参数为 a = 0.295 52 nm,b=0.295 52 nm,c=0.722 ...
2.2半定量分析步骤2.2.1查看物相标准卡片确定物相RIR值物相分析完成后,选定物相窗口中的某一 组分i选项双击Lists Pane/Pattern ListScan LiwtPeak ListAnchor ScanataQuantihcationAccepted Pattern:I ft * iFTEzza,'-No.VisibleRe/ CodeCompound NameC01 )830578Calcite匚701 08 12、9*3057Pyrite, synF3 上 00-...
The NiO obtained by the thermal decomposition of Ni (salen) sulfadiazine complex was characterised using TEM images and their SAED pattern.doi:10.1080/15533174.2015.1137038S. Jone KirubavathyR. VelmuruganB. TamilarasanR. KarvembuS. ChitraTaylor & Francis GroupSynthesis and Reactivity in Inorganic ...
It can be a good idea to label each data point on the Williamson-Hall plot according to the index of its reflection to see whether any pattern emerges. It has been stated [6], however, that the Williamson-Hall method, owing to its many assumptions, should not be taken too seriously in...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。 合图制作:命令为:file→insert *.rd scan次序调整,各scan线条颜色的设定 还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。 Highscore作图-3D(2) 数据格式的转换 Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。合图制作:命令为:file→insert*.rdscan次序调整,各scan线条颜色的设定还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。/08:05:44Highscore作图-3D(2)/08:05:44Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...
图3 A-DS和 B-DS的高温原位 XRD谱 Fig.3 In situHT-XRD patternsofA-DSandB-DS’ (a)A—DS;(b)B-DS o—Zns;▲一 Ni;口一 NiO;一一ZnO ;·一Zn2SiO4;O--ZnAI2o4;◆一zn~o(so4)2 对于 A—DS,随着温度的升高 ,归属于 Ni物相 62.82。处 出现 了峰型尖锐 的 ZnO物相 的特征衍射 的特征...
Surface EXAFS, NEXAFS and photoemission have been used to study the structure of surface phases resulting from reaction of H2S with NiO(100) and SO2 with TiO2(110). S K-edge SEXAFS data, in conjunction with the LEED pattern symmetry, sug... CA Muryn,D Purdie,P Hardman,... - 《Farada...
while littlecharge transferoccurredduringadsoprtionofPontheIOCS.AccordingtovalencebandspectraofXPS,thebindingstrengthbetweenIOCSandSbwasstronger thanthatbetweenIOCSandP.TheatomicratioofFeonIOCSdecreasedbecauseoftheoverlaybytheadsorbedantimonyandphosphate.Thesputtering resultsfurthersuggestedthatantimonycouldbeinteracted...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。 合图制作:命令为:file→insert *.rd scan次序调整,各scan线条颜色的设定 还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。 Highscore作图-3D(2) 数据格式的转换 Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...