Temperature: The approximate temperature of data collection was 26 C.Pattern: To replace 00-...
图3 A-DS和 B-DS的高温原位 XRD谱 Fig.3 In situHT-XRD patternsofA-DSandB-DS’ (a)A—DS;(b)B-DS o—Zns;▲一 Ni;口一 NiO;一一ZnO ;·一Zn2SiO4;O--ZnAI2o4;◆一zn~o(so4)2 对于 A—DS,随着温度的升高 ,归属于 Ni物相 62.82。处 出现 了峰型尖锐 的 ZnO物相 的特征衍射 的特征...
The NiO obtained by the thermal decomposition of Ni (salen) sulfadiazine complex was characterised using TEM images and their SAED pattern.doi:10.1080/15533174.2015.1137038S. Jone KirubavathyR. VelmuruganB. TamilarasanR. KarvembuS. ChitraTaylor & Francis GroupSynthesis and Reactivity in Inorganic ...
2.2半定量分析步骤2.2.1查看物相标准卡片确定物相RIR值物相分析完成后,选定物相窗口中的某一 组分i选项双击Lists Pane/Pattern ListScan LiwtPeak ListAnchor ScanataQuantihcationAccepted Pattern:I ft * iFTEzza,'-No.VisibleRe/ CodeCompound NameC01 )830578Calcite匚701 08 12、9*3057Pyrite, synF3 上 00-...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。合图制作:命令为:file→insert*.rdscan次序调整,各scan线条颜色的设定还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。/08:05:44Highscore作图-3D(2)/08:05:44Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。 合图制作:命令为:file→insert *.rd scan次序调整,各scan线条颜色的设定 还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。 Highscore作图-3D(2) 数据格式的转换 Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...
在Pattern窗口下另存为,则可以保存实验峰和标准卡片峰。 合图制作:命令为:file→insert *.rd scan次序调整,各scan线条颜色的设定 还可以将经过smooth等操作的衍射图另存为*.rd,然后再重新insert,图会漂亮很多。 Highscore作图-3D(2) 数据格式的转换 Highscore1.0是一款非常优秀的物相检索软件,但功能有限。不具备的...
A Rietveld analysis [38] was conducted to determine the phase transformation kinetics and the evolution of the dislocation density. Pictures of Debye-Scherrer (DS) rings have been integrated using the Fit2D software. The 1D diffraction pattern was then refined with Fullprof software (V2.05, ILL,...
In situ XRD characterization consists of two aspects: (1) the full-pattern scanning model in steps of 0.02 ◦ over the range 15–65 ◦. CO2 chemisorption from 50 to 850 ◦C in an 80 vol% CO2–20 vol% N2 atmosphere with a heating step of 10 ◦C·min−1. When it was 850...
In most cases, the PED patterns also go to higher resolution than an SAED pattern collected from the same crystal. Therefore, the structural information obtained using PED is more accurate. Using the diffraction intensity of the kinematical approximation in PED, the structures of some materials ...