A newly developed method allows structure elucidation of proteins inside intact mammalian cells, using solid-state NMR spectroscopy. Arunima Singh Research Highlights30 Jul 2019Nature Methods Volume: 16, P: 676 The makeup of a gamete space capsule ...
Solid-state NMR(SSNMR) is a powerful probe of the molecular-level geometric, electronic, and magnetic environment about a target nucleus. Significant advances have been made in91ZrSSNMR spectroscopysince its inception, particularly within the past 25 years.91Zr is an unfavorable nucleus for SSNMR ...
(H/D) exchange and solid-state NMR (SSNMR) to follow membrane protein unfolding in lipid membranes at atomic resolution through detecting changes in the protein water-accessible surface, and concurrently monitoring the reversibility of unfolding. We obtain atomistic description of the reversible part ...
We review here the different methodologies used to study 1H homonuclear dipolar couplings in solid-state NMR. Because most protonated powder samples contain clusters of strongly coupled 1H nuclei, structural studies based on the measurement of individual 1H homonuclear dipolar couplings have long been ...
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The order-disorder phenomenon and spatial heterogeneity of chain packing, partitions of stereodefects, and molecular dynamics of alpha form of isotactic polypropylene (iPP) samples, which are synthesized by Zieglar-Natta catalysts, are investigated by solid-state (SS) NMR. High-resolution C-13 NMR...
Solid-state NMR reveals differential carbohydrate utilization in diapausing Culex pipiens 来自 EBSCO 喜欢 0 阅读量: 33 作者:J Chang,J Singh,S Kim,WC Hockaday,C Sim,SJ Kim 摘要: Culex pipiens is the mosquito that vectors West Nile Virus and other human-pathogenic flavivruses in North America....
Here we demonstrate that magic angle spinning solid-state NMR spectroscopy can be used to determine structures of membrane proteins reconstituted in synthetic lipids, an environment similar to the natural membrane. We combined a large number of experimentally determined interatomic distances and local ...
NMR relaxometry has gained popularity in recent years, due to advances in experimental methodology and theory. We present an overview of applications of NMR relaxometry (with special focus on Field Cycling studies) to solid state, including a variety of systems ranging from simple crystals to ...
Acidity characterization of heterogeneous catalysts by solid-state NMR spectroscopy using probe molecules. Solid State Nucl. Magn. Reson. 55−56, 12–27 (2013). PubMed Google Scholar Zheng, A., Deng, F. & Liu, S. B. Acidity characterization of solid acid catalysts by solid-state 31P ...