Solid-state NMR of matrix metalloproteinase 12: an approach complementary to solution NMR. ChemBiochem, 8, 486-489.Balayssac, S. et al. Solid-state NMR of matrix metalloproteinase 12: an approach complementary to solution NMR. ChemBioChem 8, 486-489 (2007)....
nuclear magnetic resonance (ssNMR) spectroscopy is a variant of the NMR spectroscopy technique used for molecular structure determination, where the experimental sample is contained in media with little or no mobility (such as, a crystalline or powder state, membrane-bound system or aligned solution)...
摘要: The first examples of symmetrically bridging μ-perpendicular phosphaalkyne complexes are reported. Their structures have been established by solution and solid state 31P{1H} NMR spectroscopy.关键词:Phosphorus Rhodium Alkyne Nuclear magnetic resonance ...
One- and two-dimensional-solution NMR is discussed for lignin structure characterization, while solid-state cross-polarization/magic angle spinning (CP/MAS) 13C NMR is focused on analysis of the crystallinity and ultrastructure of cellulose. The solution and solid-state NMR techniques presented in ...
The P CP/MAS NMR spectra from powder samples and the P and Co solution NMR spectra of [RCo(DH) PPh ] (R=Me, n-Pr, CH Ph, CH Cl, CH CF , Ph, i-Pr) are reported. Due to coupling to Co ( I=7/2), the P CP/MAS spectra exhibit, except for R= i-Pr, distorted octets ...
RSS Feed Solid-state chemistry is the study of the preparation, structure and properties of solid materials. Latest Research and Reviews Stabilization of oxygen vacancy ordering and electrochemical-proton-insertion-and-extraction-induced large resistance modulation in strontium iron cobalt oxides Sr(Fe,Co...
A solid-state NMR method for solution of zeolite crystal structuresPOWDER DIFFRACTION DATAANGLE-SPINNING NMRX-RAY-DIFFRACTIONMAS-NMRMOLECULAR-SIEVESCRYSTALLOGRAPHYSPECTROSCOPYCOUPLINGSSILICAFERRIERITESince zeolites are notoriously difficult to prepare as large single crystals, structure determination usually relies ...
Optimum pH ranges and thermal treatment conditions have been established on the basis of extensive solution- and solid state NMR spectroscopies. The NMR spectra help identify the various types of local environments present in the sols, gels and glasses, thereby providing a mechanistic understanding of...
The comparison of solid state and solution 13C NMR spectra of the model compound trans, trans-2,5-dimethyl-1,4-bis(2-(3,4,5-trimethoxyphenyl)ethenyl) benzene showed that essentially the same conformation exists in both states. The molecule is almost planar exhibiting an ortho-methyl-syn for...
B. A proposed solution for the lifetime puzzle of the 229mTh+ isomer. Nucl. Phys. A 1010, 122173 (2021). Article CAS Google Scholar Kroemer, H. Problems in the theory of heterojunction discontinuities. CRC Crit. Rev. Solid State Sci. 5, 555–564 (1975). Article CAS Google Scholar ...