2 0 1 4 RP— HPLC— PDA 同时测定石见穿不 同部位 中 5 个三萜酸 姜琼, 邹盛勤 ( 江西省天然药物活性成分研 究重点实验 室 宜春学院 化学与生物工程学院 江西省 高校应用化 学与化学生物学重点实验 室,江西 宜春 336000) [摘要] 目的: 建立 RP— HPLC— PDA 测定石见穿不同部位中5 个三萜酸(坡...
A simple, rapid and sensitive RP-HPLC-PDA method was developed and validated as per ICH guidelines for the analysis of tapentadol in bulk as well as in tablet formulation. The RP-HPLC isocratic method was developed using a column LC-GC Qualisil BDS C-18 (250 mm 4.6 mm 5 m) and ...
目的:建立RP-HPLC-PDA测定石见穿不同部位中5个三萜酸(坡模酸、山楂酸、科罗索酸、齐墩果酸和熊果酸)的定量方法.方法:采用KromasilC18色谱柱(4.6mm×250mm,5μm),流动相为乙腈-水(90:10,体积比),等度洗脱,检测波长205nm,流速0.8mL·min-1,柱温28℃.结果:坡模酸、山楂酸、科罗
RP-HPLC-PDA同时测定中药中补骨脂素和异补骨脂素含量 作者:张海容 马晓婷 高瑞苑 基本信息来源于合作网站,原文需代理用户跳转至来源网站获取 补骨脂 补骨脂素 异补骨脂素 高效液相色谱 中药 摘要: 建立了中药中补骨脂素、异补骨脂素的高效液相色谱分析方法.采用的色谱条件为:Symmetry C18色谱柱(4.6mm×250mm,5μm),...
A simple, selective, rapid, and precise RP-HPLC-PDA method has been developed for the simultaneous estimation of Lornoxicam (LOR) and Thiocolchicoside (THIO) in pharmaceutical dosage form by reverse phase liquid chromatography using Waters Symmetry C18 (250 mm × 4.6 mm, 5.0 μ) column. ...
高智席,吴艳红,郑胡飞,敖克厚,刘焱,曾启华,黄成. 灯笼果中噻菌灵的RP-HPLC-PDA残留分析[J]. 2012.高智席;吴艳红;郑胡飞;敖克厚;刘焱;曾启华;黄成.灯笼果中噻菌灵的RP-HPLC-PDA残留分析.食品科学.2012.204-207灯笼果中噻菌灵的RP-HPLC-PDA残留分析[J]. 高智席,吴艳红,郑胡飞,敖克厚,刘焱,曾启华,黄...
A simple, rapid and sensitive RP-HPLC-PDA method was developed and validated as per ICH guidelines for the analysis of tapentadol in bulk as well as in tablet formulation. The RP-HPLC isocratic method was developed using a column LC-GC Qualisil BDS C-18 (250 mm 4.6 mm 5 m) and methan...
摘要 目的建立反相液相色谱分离二极管阵列双波长检测法测定复方泰妙林注射液中泰妙菌素、磺胺嘧啶钠的含量的方法.方法采用Shim-pack CLC-ODS柱(150 mm×6 mm,5 μm),流动相为80 %乙腈-0.7 %磷酸氢二铵(体积比为0.3:0.7),并用氨试液调节pH至8.0±0.1,流速为1.0 mL/min,泰妙菌素和磺胺嘧啶钠的检测波...
Table 3. Results from precision studies for RP-HPLC-PDA analysis of zileuton. DrugZileuton Concentration (μg mL−1)Amount found in μg mL−1 [n = 9] ± SDRSD (%) Intra-day precision 4 4.002 ± 0.009 0.23 6 6.005 ± 0.012 0.21 8 7.977 ± 0.022 0.27 Inter-day precision 4 3.997...
Development and validation of a RP-HPLC-PDA method for simultaneous estimation of Drotaverine and Aceclofenac in a combined dosage form. Int J Res Pharm Sci 2010; 1: 253-258Vishnu Choudhari, KunalIngale, MadhusmitaSahoo, et al. Development and validation of a RP-HPLC-PDA method for ...