As one example, results of quantitative MALDI-MSI can be matched to UHPLC-TQ-ESI-MS measurements performed on the same tissue. However, cross platform comparisons are affected by differences in the physical and chemical parameters of the samples, and may be aided by normalization approaches. ...
By this way, the device could nebulize the drug solutions into the simulated exhaled breath containing illicit drugs at different levels, and the collection unit with electret material could adsorb drugs in the sampled SHEBA for HPLC-TQ-MS/MS detection. Thus, this study aimed to develop, ...
Assemble and validation of a simulated device of human exhaled breath aerosols for screening of illicit drug abuse by HPLC-TQ-MS/MS detection 来自 dx.doi.org 喜欢 0 阅读量: 8 作者:L Chen,J Zhou,Y Shi,F Xu,X Liu,Q Huang,J Zhong,K Wu,D Yang,H Fan ...
To explore the nutrients in roots of Angelica sinensis (Angelicae Sinensis Radix, ASR), a medicinal and edible plant, and evaluate its nutritional value, a rapid and reliable UHP...
· kg-1)后眼底静脉丛取血,血浆经甲醇预处理后进入HPLC-TQ-MS/MS分析.用DAS统计软件计算加味败藤浸膏中活性成分的药动学参数.结果 经方法学考证,血浆中小檗碱、大车前苷、柴胡皂苷a、延胡索乙素、芍药苷和苦杏仁苷的线性范围分别为0.59~ 292.50,0.68 ~ 168.75,6.05 ~1 512.50,0.68 ~ 337.50,6.70...
By means of ultra highperformance hyphenated with triple quadrupole tandem mass spectrometry (HPLC-TQ-MS/MS), using caffeine as a target drug, the device parameters were investigated by studying the effects of flow rates of nebulizing and auxiliary gases, drug concentration and etc., the ...
Application of the HPLC-PDA-ESI-tQ-MS/MS technique led to the identification of 28 compounds, such as iridoid glycosides, flavones and xanthones, with loganic acid, sweroside, loganin, secologanin, isoorientin-7-O-glucoside, luteolin-7-O-gentiobioside, chrysoeriol-7-O-glucoside and acacetin...
Chemical Profile Determination and Quantitative Analysis of Components in Oryeong-san Using UHPLC-Q-Orbitrap-MS and UPLC-TQ-MS/MSTANDEM mass spectrometryASIAN medicineQUANTITATIVE researchLIQUID chromatographyMASS spectrometryQUADRUPOLE ion trap mass spectrometryIn this study, a method to both qualitatively ...
molecules Article UHPLC-TQ-MS Coupled with Multivariate Statistical Analysis to Characterize Nucleosides, Nucleobases and Amino Acids in Angelicae Sinensis Radix Obtained by Different Drying Methods Shaoqing Zhu, Sheng Guo *, Jin-ao Duan *, Dawei Qian, Hui Yan, Xiuxiu Sha and Zhenhua Zhu Jiangsu ...
A simultaneous quantitative method for analysis of the 22 identified compounds was established using UHPLC coupled with a triple-quadrupole tandem mass spectrometer (UHPLC-TQ-MS/MS) in multiple reaction monitoring mode. The established method was validated in terms of linearity (R2, 0.9990–0.9996)...