Solid State Reaction study has been performed on the systems Li 2CO 3–FeC 2O 4·2H 2O and Li 2CO 3–Fe 2(C 2O 4) 3·6H 2O in the composition range x Li (lithium cationic fraction) = 0.10–0.50. By means of high resolution TGA, XRD and DSC, it has been shown that, ...
To investigate the structural evolutions of Fe2(MoO4)3 during Li1 and Na1 intercalation/deintercalation, a series of synchrotron based XRD patterns were collected at different charge/discharge states. As shown in Fig. 2a for LixFe2(MoO4)3 (x 5 0.0, 0.5, 1.0, 1.5 and 2.0) during the ...
The MgFe 2 (C 2 O 4 ) 3 ·6H 2 O and its calcined products were characterized by thermogravimetry and differential scanning calorimetry (TG/DSC), Fourier transform FT-IR, X-ray powder diffraction (XRD), and vibrating sample magnetometer (VSM). The result showed that MgFe 2 O 4 ...
The thermal decomposition of FeC2O4 center dot 2H(2)O prepared by solid-state method was investigated in air using TG-DTG/DSC. The precursor and its decomposition products formed at various temperatures were characterized by FT-IR and XRD. As evidenced by the results, the thermal ...