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The deconvoluted mass spectrum revealed three masses, corresponding to the three different dimer species: 14N − 14N, 14N − 15N, and 15N − 15N. Extended Data Fig. 8 Predicted ApnU dimer. The predicted homodimer structure was constructed based on the disulfide bond pairing ...
20). These results imply the presence of triple-bond containing species such as the unreacted internal diynes or end groups in the oligomeric products. However, the aforementioned spectral signals become weaker and weaker as the monomer feed ratio of 1a and 2a gradually increases and almost ...
6. NMR Spectrum13C NMR : Predict 1H NMR : Predict 7. Computed PropertiesMolecular Weight:594.7g/mol Molecular Formula:C36H38N2O6 Compound Is Canonicalized:True Exact Mass:6 XLogP3-AA:594.27298694 Monoisotopic Mass:594.27298694 Complexity:948 Rotatable Bond Count:2 Hydrogen Bond Donor Count:2 ...
3. NMR Spectrum13C NMR : Predict 1H NMR : Predict 4. Computed PropertiesMolecular Weight:286.1g/mol Molecular Formula:C14H14FeO310* Compound Is Canonicalized:True Exact Mass:-3.4 XLogP3-AA:426.21144931 Monoisotopic Mass:426.21144931 Complexity:579 Rotatable Bond Count:5 Hydrogen Bond Donor Count:...
spectrum of ATNNs-Co, an extra Gaussian peak appears at 782.8 eV for ATNNs-Fe-Co, which suppresses neighboring peaks and broadens the Co L3-edge spectrum. The extra peak most likely results from the Co-O-Fe bonding environment,37,38,39and the broad feature suggests its influence on a ...
Samples were analyzed using triple quadrupole liquid chromatography equipment with a PDA detector (WatersTM 996) and an Ultra AQ C18 column (3 μm × 100 × 2.2 mm) coupled to a WatersTM 2695 mass spectrum. Samples were analyzed by electrospray in mode positive (ESI+) under the following ...
Phenol, a vital intermediate resulting from hydrogenolysis of aryl ether linkages, was efficiently dehydroxylated and hydrogenolyzed despite the bond dissociation energy of the C–O bond as high as 463.6 ± 4.2 kJ/mol [47] (Table 3, entry 2). As shown in entries three–five in Table 3, ...
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