The XRD pattern of the synthesized powder confirmed the formation of single-phase LiDyO2. From the TG-DTA study it was observed that the decomposition of Li2CO3 starts at 740.9°C and the reaction between Li2CO3 and Dy2O3 starts at 750°C. The XRD analysis confirmed that mass loss observed...
In situ XRD characterization consists of two aspects: (1) the full-pattern scanning model in steps of 0.02 ◦ over the range 15–65 ◦. CO2 chemisorption from 50 to 850 ◦C in an 80 vol% CO2–20 vol% N2 atmosphere with a heating step of 10 ◦C·min−1. When it was 850...