,2019 UHPLC-QqQ-MS 测定蒲地蓝消炎口服液中 12 种成分的含量 高文雅,顾欣如,赵利娟,周严严,边宝林* ,赵海誉* ( 中国中医科学院 中药研究所,北京 100700) [摘要] 目的: 建立超高效液相色谱串联三重四级杆质谱法同时测定蒲地蓝消炎口服液中汉黄芩苷,黄芩苷,汉黄芩素, 白杨素,木犀草素,咖啡酸,乙酰紫堇灵,...
The UHPLC-QQQ-MS/MS method was first developed to simultaneously determine six dianthrones in PMR and PMRP, namely, polygonumnolides C1–C4 (1–4), trans-emodin dianthrones (5), and cis-emodin dianthrones (6). The contents of 1–6 in 90 batches of PMR were in the ranges of 0.027...
㊀㊀摘要㊀目的:建立蜈蚣中核苷类成分的UHPLC-QQQ MS 检测方法,并对结果进行分析与评价㊂方法:采用UH-PLC-QQQ MS 法同时测定4个省份(安徽㊁江苏㊁浙江㊁湖北)33批蜈蚣样品中的23个核苷类成分,并对结果进行主成分分析(PCA)㊂结果:蜈蚣中含有丰富的核苷类成分,不同样品核苷类成分含量差异较大,次黄...
UHPLC-QqQ-MS测定蒲地蓝消炎口服液中12种成分的含量作者:高文雅; 顾欣如; 赵利娟; 周严严; 边宝林...蒲地蓝消炎口服液超高液相色谱串联三重四级杆质谱质量控制摘要:目的:建立超高效液相色谱串联三重四级杆质谱法同时测定蒲地蓝消炎口服液中汉黄芩苷、黄芩苷、汉黄芩素、白杨素、木犀草素、咖啡酸、乙酰紫堇灵、...
UHPLC-QQQ-MS发布时间:2021-09-16 12:37 联系我们 上海诗丹德标准技术服务有限公司 上海市中药物质基础与标准专业技术服务平台 地址:上海市浦东新区古丹路15号申江科创园25号楼 邮箱 标准物质销售:sales@nature-standard.com 技术/检测服务:tech@nature-standard.com 联系电话 400-820-0586 关注诗丹德公众号 ...
com[通信作者]*边宝林,博士,研究员,从事中药活性成分研究工作,Tel:010-84041249,E-mail:blbian@ icmm. ac. cn;*赵海誉,博士,副研究员,从事中药活性物质基础及生物学表征研究工作,Tel:010-84041249,E-mail:hyzhao@ icmm. ac. cnUHPLC-QqQ-MS 测定蒲地蓝消炎口服液中 12 种成分的含量高文雅,顾欣如,赵利娟,...
UHPLC-QQQ-MS/MS: Ultrahigh-performance liquid chromatography coupled with triple quadrupole tandem mass spectrometry WADA: World Anti-Doping Agency .https://www.usada.org/sanction/carlee-acevedo-fuller-accepts-doping-sanction/(2017). US Anti-Doping Agency. US weightlifting athlete Lazaro Roman accepts...
To assess the preclinical pharmacokinetic drug–drug interaction a rapid, simple, and sensitive approach for the simultaneous estimation of losartan and aprepitant in rat plasma by LC–QqQ-MS/MS has been developed and validated. The separation was done on Agilent ZORBAX Eclipse Plus C18 (4.6 mm ...
Fifteen polyphenolic compounds including protocatechuic acid, ferulic acid, vanillic acid, epicatechin, p-coumaric acid, cinnamic acid, eriodictyol and quercetin-3-glucoside were identified in the pulp of this species by using UHPLC-QqQ-MS/MS analysis. The total carbohydrates and crude protein ...