5 μm particle size) or equivalent columns that guarantee baseline separation for furosine without interfering with other peaks. Gradient elution was performed using solvent A (0.4% acetic acid solution) and solvent B (0.3%potassiumchloride solution) starting at 100% A. Flow rate was set to 1.2...
Kobayashi et al, “Oxygenation of Hypoxic Region in Solid Tumor by Administration of Human Serum Albumin Incorporating Synthetic Hemes”. J Biomed Mater Res; 64A:2003; 48-51. Fylaktakidou et al. “Inositol Tripyrophosphate: A New Membrane Permeant Allosteric Effector of Haemoglobin”. Bioorganic...
(minor)) as a colorless oil. The diastereomeric ratio of 2e was determined to be 90:10 by the analysis of 1H-NMR. Major diastereomer; The enantiomeric purity of the title compound was determined by HPLC analysis (DAICEL CHIRALPAK IE-3, hexane: 2-propanol = 200: 1, flow rate = 1.0 ...