Crystal structure of 2-(l-phenylselenonyl-l-phenylethoxy)ethanol, Ci6Hi804SeCi6Hi804Se, monoclinic, P\\\2\\\k\\\ (No. 14), a = 9.831(6) A,b = 17.720(8) A, c = 9.706(6)...
Crystal structure of triaqua-bis(2-(6-hydroxy-5-(hydroxymethyl)-5,8a-dimethyl-2-methylenedecahydronaphthalen-1-yl)-1-(2-oxo-2,5-dihydrofuran-3-yl)ethane-1-sulfonato-κ2O,O′)calcium(II) – ethanol (1/2), C44H76CaO19S2 The crystal structure of ethyl 5-(4-(diphenylamino)phenyl)...
Synthesis, Structure, and Reactivity of a 2,3-Dialuminated Indole Derivative 1-Methylindole was dimercurated upon treatment with mercuric acetate (2 equiv) in 1:1 ethanoldiethyl ether to afford 2,3-bis(acetoxymercurio)-1-methylindol... CE Reck,A Bretschneider-Hurley,MJ Heeg,... - 《Organome...
In the present work, we used the Knoevenagel condensation under catalyst-free conditions for the condensation reaction of 2-picoline and benzaldehyde which allowed us to obtain the 1-phenyl-2-(2-pyridyl)ethanol compound and the dehydration compound 1-phenyl-2-(2-pyridyl)ethene (Scheme 1). The...
The structure was refined by least-squares techniques to a conventional R-factor of 10.0% using 2804 reflections, collected using a four-circle diffractometer, for which F2 ⩾ σ(F2). The ethanol of crystallisation was highly disordered, and a satisfactory description was not obtained for it. ...
2(1-Phenyl-3一methyl一5-chloro—IH—pyrazol一 4一y1)-3一(1.naphthoylamido).4.thiazolidinone① LIMing’ 一 WENLi—Rong J GShu.Xia ZHAOGui—Long。 YANGHua—Zheng。 (InstituteofElemento—organicChemistry,NankaiUniversity, in30007l,China) ”(CollegeofChemistryandMolecularEngineering, QingdaoUniversi...
The crystal structure of (Z)-3-((2-(2-(2-aminophenoxy)ethoxy)phenyl)amino)-1-phenylbut-2-en-1-one, C24H24N2O3 C24H24N2O3, monoclinic, P21/n (no. 14), a = 13.674(3) , b = 7.3900(14) , c = 20.862(4) , β = 106.728(7)°, V = 2018.9(7) 3, Z = 4, Rgt(F) = ...
A variety of [Ru(CO) 2 L(η 4 enone)] complexes (L = phosphines, phosphites, and arsines, enone = ( E )-4-phenylbut-3-en-2-one) have been synthesized. 1 H-, 13 C-, and 31 P-NMR spectra are reported and the X-ray structures of two Ru complexes with L Ph 3 P(7), ...
A mixture of naphthalene-1,8-diamine (1.58 g, 10 mmol) and 4-bromobenzaldehyde (1.85 g, 10 mmol), in anhydrous ethanol (50 mL) was refluxed at 353 K for about 2 h. Then the solvent was removed under reduced presure. The resulting residue was purified by recrystallization from ethanol ...
Crystal and Molecular Structure of Bis[2-( pheny1azo)phenyl-C1 N']gold( 111) Tetrach loroau rate t Jose Vicente,' Maria-Teresa Chicote, and Maria-Do... José,Vicente - 《Dalton Transactions》 被引量: 0发表: 1984年 cis-Dichlorobis(4,5-diazafluoren-9-one-κ2N,N′)manganese(II) ...