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The mixture of Li2S (Mitsuwa Chemical (Cavite, Philippines), 99.9%) and P2S5 (Aldrich (St. Louis, MO, USA), 99%) was put into a ZrO2 pot (volume = 45 mL) with 4 mm diameter ZrO2 balls (500 balls), and was ball-milled in a PULVERISETTE (Fritsch, Idar-Oberstein, Germany) at ...