The Ca/Si atom ratios in the ITZs of IOTs concrete samples are lower than those of limestone concrete; the diffraction peak of the calcium silicate phase at 2 胃 = 29.5掳, as well as the bands of Si-O bonds shifting to lower wavenumbers, indicates reconstruction of the broken Si-O-Si...
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The intensity and spectral position of the LO peak, observed upon silanization of a variety of silane molecules, are shown to be reliable fingerprints of formation of interfacial bonds that effectively extend the Si−O network after SAM formation. While the IR absorption intensities of functional...
Infrared spectroscopy (IR) is the most widely used analytical tool to quantify trace water in silicate and silica minerals. A prerequisite for highly accurate IR measurements of trace water is a good understanding of the effect of the second Si–O vibrational overtones/combination bands (2nd Si–...
The former excited peak is ascribed to 4f 8–4f 75d transition of the Tb3+ ion, while the latter peaks are from the intra-4f 8 transitions45,46. Under the excitation wavelength of 268 nm or 378 nm, the NwabhasBiocarhp3Ltciaao3nnSibi6sOea2a0fs:o0crr.b2ibi0de Tddbetn3...
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With the increase in temperature, the peak of Al-Si spinel was enhanced and then disappeared in the XRD pattern, and the characteristic IR band groups of mullite centered in the 1 200~1 100, 1 000~700 and 650~400 em-1 could be observed. At 1 100~1 150 ℃,the Raman bands at ...
CV of the modified electrode in presence of dilute ginger solution showed a distinct surface-confined redox peak at E1∕2, 490±20 mV vs Ag/AgCl with peak-to-peak separation and surface-excess values of 60±2 mV and 20.66×10−9molcm−2 respectively. Physico-chemical characterizations of...
While Al–O peak at 744 cm−1 and Zn–O peak is at 570 cm−1. Thermo gravimetric analysis (TGA). TGA was done by using thermal analyzer TA SDT Q600. Figure 3a shows the thermo gravimetric analysis of uncalcined sample of Zinc aluminosilicate. Derivative of TGA curve was ...
The dominant OH-vibration visible in the IR-spectrum of H2Si2O4 indicates the presence of silanole-groups, and is not related to absorbed water. Comparing the two structure factors it becomes evident that the peak positions do not differ. The peaks of the structure factor of H2Si2O4 are ...