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XRD. A four-circle x-ray diffractometer (PANalytical Xpert Pro MRD) with a Cu source and a 4-bounce hybrid monochromator was used to give pure K-a1 radiation (l 5 1.540598 A˚ ). A Pixcel detector was used in scanning mode to collect the 2h 2 v diffraction scans. The reciprocal ...