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This process is demonstrated for different metals (Pt, Pd, Cu, and Ru) and can probably be extended to other metals. Moreover, as no reducing agent is necessary (the decomposition in an argon atmosphere at 50 ˝C is fostered by surface silicon hydride groups borne by PSi), the safety ...
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3.1.3. Method C A solution of the carbamate (115 mmol) in 72 mL Ac2O was added slowly with stirring to a cooled (5–10 ◦C) suspension of finely-ground Cu(NO3)2·(H2O)3 (10.5 g; 43 mmol) in 85 mL Ac2O. After 1 h, an additional portion of finely-ground Cu(NO3)2·(H2O)...
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