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The direct 纬-C(sp3)鈥揌 activation of saturated 伪-keto esters has long been an elusive transformation. We found that photoredox catalysis involving IrIII in combination with DABCO as a dual hydrogen-bonding donor and organic base can lead to the transient generation of the multi-蟺-electron ...
ChemInform Abstract: Redox-Neutral α-Oxygenation of Amines: Reaction Development and Elucidation of the MechanismCyclic secondary amines and 2-hydroxy-benzaldehydes or related ketones react to furnish benzo[e][1,3]oxazine structures in ... Richers, Matthew T.,M Breugst,Platonova, Alena Yu.,.....
of TfPy[OTf] after varying reaction times. The ongoing deoxygenation of intermediate 4 (δ(31P) = –17.5 ppm) to phosphinate 1+ (δ(31P) = –15.2 ppm) is observed. Extended Data Fig. 3 31P{1H} NMR spectra (CH3NO2, C6D6-capillary, 300 K) of the reaction of H3PO...
C-Cbondformationcatalysisphase-transfercatalysisringA novel Rh(III)-catalyzed regioselective and redox-neutral annulation reaction of 1-naphthylamine N-oxides with -diazomalonates is developed.doi:10.1002/chin.201608140BingZhouZhaoqiangChenYaxiYang
goldSelectivity is golden: The first asymmetric redox-neutral domino reaction catalyzed by gold that results in the direct functionalization of unreactive sp(3) C-H bonds has been reported. This method consists of a heterocyclization/1,5-hydride transfer/cyclization reaction and provides synthetically...
et al. The role of TiO2 doping on RuO2-coated electrodes for the water oxidation reaction. J. Phys. Chem. C 117, 6126–6135 (2013). Article Google Scholar Jiao, Y., Jiang, H. & Chen, F. RuO2/TiO2/Pt ternary photocatalysts with epitaxial heterojunction and their application in CO ...
A low-cost manganese-catalyzed oxidant-free selective C–H acylation of indole with ketene is reported. This protocol features mild reaction conditions and good functional group tolerance. The yield is from middle to excel
et al. The role of TiO2 doping on RuO2-coated electrodes for the water oxidation reaction. J. Phys. Chem. C 117, 6126–6135 (2013). Article Google Scholar Jiao, Y., Jiang, H. & Chen, F. RuO2/TiO2/Pt ternary photocatalysts with epitaxial heterojunction and their application in CO ...
and high reaction temperatures which improved the reaction’s environmental friendliness as well as reduced the complexity and cost associated with the whole synthetic process. Therefore, the method’s efficiency and mild reaction conditions make it suitable for a wide range of applications, potentially...