2 were directly reacted in a calorimeter, the reaction energy, expressed as the total reaction heat ▵H, could be obtained. However, if the same reaction was carried out in the same calorimeter by using the fuel cell device shown inFig. 1.1, two parts of the reaction energy could be ...
DSC tests were performed on a Mettler Toledo (Columbus, OH, USA) TA4000 calorimeter between room temperature and 500 °C with heating rates of 10 °C/min under a N2 atmosphere [35]. The ESR spectra were recorded on a Jeol JES-FE/3X-ESR spectrometer (Jeol, Tokyo, Japan) upgraded for ...