Cu2+ions in the postreaction solutions were firstly removed via electrodeposition to avoid interference on NMR signals due to their paramagnetism61. The NMR sample was prepared by mixing 500 µL of the processed solution with 100 µL of D2O (Sigma-Aldrich, 99.9 atom...
6. NMR Spectrum 1H NMR : parameter in CCl4 7. Synthesis Route 74-98-6Total: 427 Synthesis Route 56-81-5 986 Suppliers 71-23-8 243 Suppliers 74-98-6 100 Suppliers 75-30-9 55 Suppliers 74-98-6 100 Suppliers 79-29-8 46 Suppliers View all 8. Precursor and Product prec...
A complete analysis of the proton AA′BB′ spectrum of 1,1,1,3-tetrachloropropane was carried out by the methods of homo-(INDOR) and heteronuclear 1 H{D} double resonance, with an electronic-computer calculation of the spectra according to an iteration program for the two working frequencies...
To further probe the specifics of C3F6adsorption at Hδ+sites within MFA, we recorded in situ diffuse reflectance FT-IR spectra under a pure C3F6atmosphere at 30 °C (Fig.4e). Upon exposure to C3F6, the infrared spectrum exhibited time-dependent changes, with two distinct C-F stretchin...
NMR Spectrum Computational chemical data Realated Product Infomation1. Names and Identifiers1.1 Name 1-Bromo-2,3-epoxypropane 1.2 Synonyms (±)-(Bromomethyl)oxirane; (±)-3-Bromo-1,2-epoxypropane; (±)-Epibromohydrin; (Bromomethyl)ethylene oxide; (Bromomethyl)oxirane; 1,2-Epoxy-3-bromopropane...
View entire compound with spectra: 2 NMR, 3 FTIR, and 1 MS (GC) SpectraBase Compound ID 5myrdRSVXOA InChI InChI=1S/C5H12O2/c1-5(7-3)4-6-2/h5H,4H2,1-3H3 InChIKey LEEANUDEDHYDTG-UHFFFAOYSA-N Google Search Mol Weight 104.15 g/mol Molecular Formula C5H12O2 Exact Mass ...
The Py-IR spectrum was measured on an IS-10 FTIR spectrometer instrument (Thermo Fisher Scientific). The procedure for pyridine adsorption is as follows: prior to experimental records, a self-supported wafer of the sample was pretreated at 400°C for 1 h under a vacuum. Then, after cooling...
1,2,3-Trichloropropane Spectrum 1,2,3-Trichloropropane(96-18-4)MS1,2,3-Trichloropropane(96-18-4)1HNMR1,2,3-Trichloropropane(96-18-4)13CNMR1,2,3-Trichloropropane(96-18-4)IR11,2,3-Trichloropropane(96-18-4)Raman 96-18-4(1,2,3-Trichloropropane)Related Search: 1-Chloropropane ...
The proton NMR spectrum of 31 has a singlet at δ 3.56 with an intensity of 2H. This singlet has a long range correlation to a carbon at δ 177.9, consistent with an amide. In addition, a nuclear Overhauser enhancement (nOe) occurs between H3 and H9. Compound 32 was found in plasma ...
to give the title compound (22.0 g, 49.92 mmol): 1H NMR (CDCl3)δ 0.58 (d, J=8.8 Hz, 3H), 1.02 (m, 3H), 1.06 (m, 1H), 1.48 (s, 9H), 3.16 (m, 2H), 3.58 (m, 4H), 3.91 (s, 3H), 5.24 (m, 2H), 6.78 (m, 3H), 7.36 (m, 5H); and 13C-NMR (CDCl3)δ (...