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o.n. before it was quenched by addition of 500 μL HOAc and 500 μL H2O and subjected to RP-HPLC purification to obtain 145 mg (0.31 mmol) of the desired product in 30% yield. The final compound was soluble up to 20 mg/mL in D2O. 1H NMR (400 MHz, D2O): δ [ppm] = 7.74 ...
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