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one-pot processThe copper(I)-exchanged zeolite Cu-I-USY proved to efficiently catalyze the direct azidation of arylboronic acids with sodium azide under simple and practical conditions, namely at room temperature under air with methanol as solvent and without any additive. This easy-to-prepare ...
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Interestingly, the azidation reaction has been successfully coupled to a CuAAC reaction, thus allowing access to triazoles from arylboronic acids via a one-pot Cu-I-catalyzed process.Clerc, ArnaudBeneteau, ValeriePale, PatrickChassaing, Stefan...
crystal structureone-dimensional chaincopper complexazobispyridineTwo copper complexes [Cu(TTA)2(4,4′-azpy)] (1) and [Cu-(TTA)2(3,3′-azpy)] (2) (HTTA = 1,1,1-trifluoro-3-(2-thenoyl)-acetone, 4,4′-azpy = 4,4′-azobispyridine, 3,3′-azpy = 3,3′-azobispyridine) ...