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The solvents used for this were n-heptane (Sigma-Aldrich Chemie GmbH, LiChrosolv HPLC grade) or methanol (J.T.Baker, Ultra HPLC Grade). HPLC. All HPLC separation were conducted with an UltiMate 3000 HPLC system (Thermo Fischer Scientific, Bremen, Germany) housing a binary pump, column ...