Eluting with ethyl acetate, methanol, and chloroform (1:1:48) pure title product. EXAMPLE 18 9-Deoxy-PGD2 Refer to Chart I. A. Following the procedure of Example 17, the reaction product of Example 16, part A is dehydrated to yield 9,10-didehydro-9-deoxy-PGD2, 15-tetrahydropyran...
ethyl 1-benzyl-... 53977-02-9 ~75% 3-Quinolinecarb... 35975-86-1 文献:Stern, Eric; Muccioli, Giulio G.; Bosier, Barbara; Hamtiaux, Laurie; Millet, Regis; Poupaert, Jacques H.; Henichart, Jean-Pierre; Depreux, Patrick; Goossens, Jean-Francois; Lambert, Didier M. Journal of Medic...
(R)-4-(4-piperidylidene)-9,10-dihydro-4H-benzo-(4,5)-cyclohepta(1,2-b)thiophene-10-one ((R)-Norketotifen): Cadmium dust (178 mg, 1.59 mmol) and a 10% cadmium/lead couple (356 mg, 3.174 mmol) were added to a rapidly stirring mixture of trichloroethyl carbamate (279 mg, 592 ...