95,96 Mg-air batteries have also found applications in military field, as the hybridization of Mg-air batteries with Ni–Zn batteries has been proposed as detector energy providers that can provide 25 kW of power for two weeks.76 In general, current Mg-air batteries are primary batteries...
DRIFTS spectra were acquired with a Bruker Vertex 70 instrument equipped with a Pike DiffusIR cell attachment and a MCT detector. Spectra were recorded carrying out 128 scans in the spectral region of 4000–600 cm−1 with a resolution of 4 cm−1. The spectra were recorded as follows: ...
The EPMA detector is present as an upgrade to conventional SEM, but most of the instruments come at least with the EDS detector by default. The electron bombardment of the beam excites the atoms in the sample, knocking out the electrons from the inner shells. Such a state is unstable, and...
The single-crystal X-ray diffraction dataset for the single crystals of 4 were collected at the “Belok/XSA” beamline [50,51] of the Kurchatov synchrotron radiation source (National Research Centre “Kurchatov Institute”), equipped with a Rayonix SX165 CCD detector (λ = 0.79475 Å, φ-sc...
The products were monitored using a Shimadzu gas-chromatography with a capillary column and detected by an FID detector. The aliquots of the liquid products were withdrawing at each 60 min intervals. The reaction products were analyzed by Intercrom Geração 8000 apparatus, and ortho-xylene used...
using either APEXII Bruker AXS diffractometer (graphite monochromator; compounds 1e, 2l, 3g, 3g′, 3k′, 4e, 4h, 4i and 5i), or D8 VENTURE Bruker AXS diffractometer equipped with a (CMOS) PHOTON 100 detector (multilayer monochromator; compounds 1e, 1i, 1j, 2k, 3a, 3a′ and 4c). ...
A PANalytical X’Celerator detector based on Real Time Multiple Strip technology and capable of simultaneously measuring intensities in the 2θ range of 2.122° was used. The XRD spectra of the virgin ZIF-8, rubber mix, and vulcanizate containing the MOF were compared in order to check their...
Measurements were taken using a glancing angle of incidence detector at an angle of 2◦, for 2θ values over 10–90◦ in steps of 0.026◦ with a step time of 37 s and at a temperature of 25 ◦C. Raman spectroscopy experiments were performed on a J-Y T64000 micro-Raman ...
The detection limit of oxygen was at a partial pressure of 10−13 mbar using a multichannel plate detector and filaments of thoriated iridium. The chamber was designed as a vertical two-zone oven, in which the “park position” of the sample was heated permanently to 300 °C, whereas the...
This PXRF instrument is equipped with an Au anode as the excitation source and a silicon drift detector, and operates at 40 kV and 0.1 mA [11]. The quantification was conducted by the software embedded in the PXRF instrument. The Compton normalization method was used as a calibration method ...