The sample pH was adjusted to 12.0 and 10% NaCl was added in the samples in order to increase the ionic strength. The method was completely validated according to Guideline on Bioanalytical Method Validation. Finally, therapeutic drug monitoring capability of the new bioanalytical method was ...
10 control and 15 ME/CFS stored platelet-poor plasma (PPP) samples were used for the proteomics analysis. Protein determination was performed using a Jenway 7415 Nano Micro-Volume Spectrophotometer. Samples were diluted 20× with ammonium bicarbonate. 50 µg of protein was obtained from each sam...
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For L = P(OEt)3, CO loss is observed to generate a separate isomer of the unsaturated species, which upon thermal reaction with CO produces cis-(η5-C5H5)Mo(CO)2P(OEt)3Me. The photoreaction of cis-(η5-C5H5)Mo(CO)2LMe, (L = PPh3, PBu3) is not CO loss but loss of L from...
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