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Bottom (lipophilic) layer was transferred to a glass vial and dried under a gentle stream of N2. The sediment was reconstituted in 180 µL of CDCl3 (0.03% v/v tetramethylsilane (TMS):CD3OD (2:1) and transferred to a 3 mm-NMR tube. 2.4. 1H NMR Spectral Acquisition and Analysis ...