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and the optimum conditions of detecting ethyl carbamate in liquor were obtained as follow: for LLE extraction, 5 m L sample were filled accurately in a 10-m L colorimetric tube spiked with PC as the internal standard, then solid K2HPO4 was added gradually until it saturated with K2HPO4 and...
However, with the most selective LC-UV method (XTerra method), two more degradation products (UNK2 and UNK3) were found in the formulation which could not be observed using other methods because of their poor separation. By combining the results obtained with LC-UV, LC/MS and LC/NMR, ...
Blood samples were collected in the tubes containing K2 EDTA (BD Biosciences, 366643), and plasma extraction was performed within 1–6 h of the blood draw. Whole blood was centrifuged for 10 min at 1,500gand 4 °C. Supernatant was transferred to a new conical tube and subjected to...
To verify the effect of temperature (T), the water mass fraction of the solvent (w4s), and the fatty acid mass fraction in the oil phase (w2OP) on the distribution coefficient of the oleic acid (k2), a complete second-order model was fitted with a determination coefficient value higher...
A tiltable trough 30 may be provided, pivotally supported on arms 31 on the trolley, by which the coating medium may be applied in advance of the air doctor 8, or it may be poured on manually. After the coating material has been applied, the air doctor 8 is traversed across the ...
A microscopic determination of κ for the stripe phase is unfortunately very complicated and beyond the scope of the present paper. We have therefore adopted a pragmatic approach simply choosing the value κ = 3 in Fig. 6, which is intermediate between the values of two microscopic models: ...
A long-range Infinity K2 Distamax microscope was mounted on a 29 megapixel CCD camera (TSI Inc., pixel pitch of 5.5 μm) at a working distance of 1.2 m from the spray axis, for a depth of focus of approximately 2 mm. This type of long-range microscope was characterized for its ...
Standard Practice for Preparation of Insulating Paper and Board Impregnated with a Liquid DielectricAstm
Differential thermal analysis in hydrostatic apparatus yielded for K2CO3: solid-liquid transition (905 ± 2°C intercept at 1 bar), 20.2 ± 0.6 deg kbar-1 slope and solid-solid (421 ± 2°C), 16.8 ± 0.8 deg kbar-1, to 5 kbar; Na2CO3: solid-solid (485 ± 3°C), 15.5 ± 0.5...