The solution was diluted with 36 mL water (285 mL/mol Cr03) and cooled to 0oC. A solution of the alcohol (19.2 g, 0.128 mol) in acetone (80 mL) (600mL/mol CrO3) was cooled to 0oC and the Jones reagent added slowly, maintaining a temperature <20oC. Stirring was continued for 3...