图1 为微通道反应器连续制备不同Cu2+浓度的HKUST-1 的XRD 图。 图1 微通道反应器合成HKUST-1 的XRD 图Fig.1 XRD pattern of prepared HKUST-1 in microchannel reactor 从图1 中可以看出,微通道反应器制备得到的HKUST-1 样品与由 HKUST-1 单晶数据模拟得到的XRD 衍射峰完全吻合,且与文献中报道的传统...
The XRD pattern of HKUST-1/LaNiO3 shows peak at 8.258° (011), 11.302° (002), 12.356° (112), 14.365° (022), 15.984° (013), 17.565° (222), 21.682° (114), Conclusion In summary, LaNiO3 decorated HKUST-1 composite was synthesized and utilized as a highly efficient pseudocapacitor...
The characteristic XRD pattern of HKUST-1 is clearly retained after the compression of the powders (Fig. 4a and b). The peak positions in the compressed materials are slightly shifted to higher angles, implying a decreased interplanar distance. Peak widening and baseline increase however indicate ...
1 20 30 40 0 0.2 0.4 0.6 0.8 1.0 2θ/(°) (a)X-射线衍射图谱 相对压力(p/p0) (b)N2吸附-解吸等温线 图 1 不同晶格空位量 HKUST-1 样品的 X-射线衍射图谱和 N2 吸附-解吸等温线 XRD pattern and N2 adsorption-desorption isotherms of HKUST-1 samples with different lattice vacancy HKUST-1...
0.566, 0.256, and 0.170 nm, respectively. This is an indication that the prepared MoS2was in pure phases. The XRD pattern of the synthesized HKUST-1 possessed diffraction peaks at 7.72, 11.27, 13.63, 15.84, 17.19, 17.60, 318.94, 20.26, 22.18, 23.65, 24.83, 26.75, 28.08, 30.29, 34.27, ...
图2 室温合成HKUST-1的SEM图(a,b)、XRD图(c)和FTIR 谱图(d)Fig.2 SEM spectrum(a,b),XRD pattern(c) and FTIRspectrum(d) of room temperature synthesized HKUST-1 将所合成的HKUST-1在120 ℃真空条件下活化2 h后用于N2吸脱附实验。所得的N2吸脱附曲线见图3。 图3 HKUST-1的N2吸附-脱附等温线...
These will include, but not be limited to, separation of mixtures, gc-ms, lc-ms, atomic spectroscopy and elemental analysis, IR and UV spectroscopy, electrochemistry, NMR, powder XRD. Students must attend and write up experimental reports for at least eight laboratory sessions to complete the ...
HKUST-1 both for S. cerevisiae and G. candidum indicates a strong inhibitory effect caused by the MOF. In order to try to establish the mode of antifungal action, physicochemical studies were conducted. 3.2. Physicochemical studies Fig. 2a shows the XRD pattern of HKUST-1 simulated fromcrys-...
1a, XRD pattern of the pristine HKUST-1 was in good agreement with the previous report [26], indicating the successful synthesis of HKUST-1. While the regenerated samples showed weaker intensities of diffraction peaks than the pristine one. It can be ascribed to the influence of adsorbed Ce3...
Fig. 1. XRD pattern of Cu2O. 3.2. The growth process and mechanism of Cu2O@HKUST-1 The key to successfully constructing nano core-shell hybrid materials using the “bottle around ship” method is to precisely match the dissolution rate of metals or metal oxides in the reaction system with ...