The MS transferline was set at 290 °C. The analytes leaving the capillary column were ionized via electron impact at 70 eV at an ion source temperature of 280 °C. Mass spectra were acquired in full scan (40–800m/z) for qualitative and quantitative analysis. The measurement results were...
Using Xcalibur software version 2.1 (Thermo Scientific, San Jose, CA, USA), a comparison was made of the mass spectra corresponding to each peak observed in the chromatogram with data obtained by the NIST library (National Institute of Standards and Technology), considering the level of ...