Then, 2.7 g de FeCl3·6H2O was added and, once it was totally dissolved, 1.06 g of FeCl2·4H2O was added to the mixture. To synthesize this sample, N2 was bubbled through the solution during the precursor's addition to reduce the presence of oxygen as much as possible, which produces...
The latter underwent complexation with FeCl3 as an anionic NNN-pincer ligand coordinating the Fe(III) by one short Fe–N(s-triazine) and two equidistant Fe–N(pyrazole) bonds. The hexa- coordination environment was completed by two chloride ions and one methanol. The [Fe(BPT)Cl2(CH3OH)] ...
Balouria, V.; Kumar, A.; Samanta, S.; Singha, A.; Debnath, A.K.; Mahajan, A.; Bedi, R.K.; Aswal, D.K.; Gupta, S.K. Temperature Dependent H2S and Cl2 Sensing Selectivity of Cr2O3 Thin Films. Sens. Actuators B 2013, 181, 471–478. [CrossRef] 14. Liu, Z.; Lv, B....
For the case of Hg2+ detection, HgCl2 solution was used instead of FeCl3. 3. Results 3.1. Spectral Properties of SQ The synthesis of sensor SQ was followed as reported literature [48] and the characterization for the compound was summarized in Figures S1–S3. The product was distinct from ...
N-doped carbon prepared by pyrolysis of dicyandiamide with various MeCl2·xH2O (Me = Co, Fe, and Ni) composites: Effect of type and amount of metal seed on oxygen reduction reactions. Appl. Catal. B Environ. 2012, 119–120, 123–131. [CrossRef] 9. Muthukrishnan, A.; Nabae, Y.; ...
The resulting black suspension was ultrasonically mixed with PdCl2 (35 mg) ethanol solution (3 mL) for 1 h, then an ascorbic acid ethanol solution (8 mL) was dropped into the above mixture with vigorous stirring under 60 ◦C. After 2 h of reduction, the products were separated by a ...
In a typical synthesis, 9 mmol of H2BDC, 6 mmol of FeCl3·6H2O, and a certain amount of Ni(NO3)2·6H2O were dissolved in 60 mL DMF. The obtained mixture was vigorously stirred for 30 min before being transferred into a 100 mL hydrothermal synthesis autoclave reactor 304 stainless steel...
Materials CuCl2, AgNO3, Mn(NO3)2, MgCl2, NiCl2·6H2O, CdCl2, Pb(NO3)2, FeCl3·6H2O, FeCl2·4H2O, 25–28% NH3·H2O, HCl, NaOH, KCl, sodium citrate, gold chloride tetrahydrate (HAuCl4·4H2O), dopamine hydrochloride (DA·HCl, 98%), mercaptopropionic acid (MPA) of analytical grade...