DSC analysis of 1) raw, 2) liquid nitrogen-treated and 3) pulverized PET samples was conducted in a Q2000 DSC (TA Instruments) to understand the impact of the downsizing process on the thermal history and polymer properties. Samples were weighed, sealed in aluminum Tzero® crucibles, and lo...
DISC TGA DSC
DISC TGA DSC
Q2000: 60 Discovery DSC: 90 1 mg 铟,10 ℃/min 氮气吹扫 163 -12 -10 -4 -6 -8 -2 0 热 流 ( m W ) 2 温度( C) 60 65 70 75 80 85 90 95 -14.0 -8.0 -10.0 -12.0 -6.0 -4.0 -2.0 热 流 ( 归 一 化 ) ( W / g ) 0 -50 温度( C) Cp文献值 0 50 100 150 200 25...