本研究拟建立血液中地芬尼多与苯海拉明的超声辅助离子液体-分散液液微萃取(ultrasound-assistedionic liquid dispersive liquid-liquid microextraction, UAIL-DLLME )-液相色谱串联质谱检测方法( liquidchromatography- tandem spectrometry, LC-MS/MS),为地芬尼多与苯海拉明相关案件的法医学鉴定提供参考。以 1-丁基-3-...
试验建立了分散液相微萃取技术和高效液相色谱-串联质谱联用快速分析食用油中5种黄曲霉毒素的新方法.食用油样品先用正己烷溶解分散,再用一定比例的乙腈和水萃取,振荡漩涡离心后LC-MS/MS测定.试验对影响萃取效果的因素进行了优化,在优化试验条件下,方法的线性范围为0.06～10μg/kg,检出限为0.02～ 0.03 μg/kg,相...
Development of multiresidue DLLME and QuEChERS based LC–MS/MS method for determination of selected neonicotinoid insecticides in honey liqueur[J] . Pavle Jovanov,Valéria Guzsvány,Mladen Franko,Sanja Lazi?,Marijana Saka?,Ivan Milovanovi?,Nata?a Nedeljkovi?.Food Research International . 2014...
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DLLME-LC-MS/MSHuman plasmaTherapeutic drug monitoringRisperidone is an antipsychotic drug commonly used in the treatment of schizophrenia and other psychiatric illnesses. Its main metabolite, 9-hydroxyrisperidone, also called paliperidone, exhibits pharmacological activity similar to risperidone, and the ...
RP-LC-PDABackground Daclatasvir is a direct-acting antiviral agent against hepatitis C virus (HCV) used for the treatment of chronic HCV genotype infections of 1 and 3. Hepatitis C is an infectious liver disease caused by infection with hepatitis C virus (HCV). There are no reports found ...
Zhao X, Fu L, Hu J, Li J, Wang H, Huang C, Wang X (2009) Analysis of PAHs in water and fruit juice samples by DLLME combined with LC-fluorescence detection. Chromatographia 69: 1385-1389Zhao XN, Fu LY, Hu J, Li JW, Wang HL, Huang CJ, Wang XD (2009) Chromatographia 69:1385...
A rapid, simple, inexpensive, and reliable vortex-assisted dispersive liquid-liquid microextraction (VA-DLLME) method was developed for the determination of fipronil and its major metabolite, fipronil sulfone, in tomato fruits using liquid chromatography tandem mass spectrometry (LC-MS/MS). No ...