9). We see a small reduction peak between −1.1 and –1.3 V in the LSV curve after adding 0.1 mmol of 1a into anhydrous N,N-dimethylformamide (DMF) solvent by using tetrabutylammonium tetrafluoroborate (TBAPF4) as the electrolyte, revealing the electron transferring from the LC-Fe ...
Solvent delay was set to 5 min. 4.4. Data Processing LC–MS data was processed with XCalibur 4.0 and Compound Discoverer 3.3 software (Thermo Scientific, Inc.) and with MS Dial [72,73]. A common routine including peak picking, deconvolution and deisotoping was used to detect components. ...
If multiple scattering occurs for a given particle/solvent system, it attenuates scattering of the incident beam that should be going in a given (forward) direction and, therefore, distorts the signal which would have been recorded in the limit of single scattering. It follows that the ...