我测的XRD只有TXT格式，是用jade6打开的，不能用mecury打开，那怎么对晶面呢？这是我参考文献做的XRD...
A composite β-mCoPc/Cu-BDC is developed by decorating Cu-BDC with β-m-phthalocyanine cobalt (β-mCoPc) and systematically investigated by a series of combined analyses of X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared (FT-IR), N2 ...
采用X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)及N2吸附-脱附技术等对分子筛进行了表征。结果表明,复合分子筛形态规整,Beta与MCM-22分别作为核壳而共生;Beta/MCM-22复合分子筛孔结构性质介于MCM-22、Beta分子筛之间。在酸性分布上,复合分子筛的中强酸及B酸所占比例* 增加(CB/CL=13.8)。通过Ar-H2等离子体...
以2-氨基对苯二甲酸,4,4′-联吡啶配体和硝酸铜为原料,在溶剂热的条件下,合成了一种的阴离子型三维金属有机框架(MOF)材料Cu(BDC-NH2)(4,4′-Bipy)0.5(BDC=对苯二甲酸根,Bipy=联吡啶).通过IR,XRD,SEM,TG,N2吸附法测比表面积等技术手段表征材料的结构和性能.研究了Cu(BDC-NH2)(4,4′-Bipy)0.5... ...
以2-氨基对苯二甲酸、4,4′-联吡啶配体和硝酸铜为原料,在溶剂热的条件下,合成了一种的阴离子型三维金属有机框架(MOF)材料Cu(BDC-NH2)(4,4′-Bipy)0.5(BDC=对苯二甲酸根,Bipy=联吡啶).通过IR、XRD、SEM、TG、N2吸附法测比表面积等技术手段表征材料的结构和性能.研究了Cu(BDC-NH2)(4,4′...
在浸泡12小时后,趋于稳定,此时的XRD谱图和模拟的1D Cu-BDC谱图类似。1D Cu-BDC的傅里叶变换红外(FTIR)光谱显示DMF的C−N(1107 cm−1和676 cm−1)和C=O(1663 cm−1)振动消失,同时保持BDC配体的苯环带(1386 cm−1、1154 cm−1和1018 cm−1)。此外,在2900 cm−1–3700 cm−1出现水...
According to XRD spectra, the composition of the main chemical bonds in the Cu-BDC-NH2 MOF samples should be maintained. In the wavenumber region from 4000 to 500 cm−1 (Figure 1e), the presence of a Cu-O stretching vibration was indicated by the distinctive and strong absorption band ...
According to XRD spectra, the composition of the main chemical bonds in the Cu-BDC-NH2 MOF samples should be maintained. In the wavenumber region from 4000 to 500 cm−1 (Figure 1e), the presence of a Cu-O stretching vibration was indicated by the distinctive and strong absorption band ...
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Cu@FSL-1中的Cu NPs是与I2进行电荷转移的主要活性位点(图6c),这与XRD和XPS的分析结果一致。此外,为了进一步了解吸附碘分子与母体FSL-1的相互作用,进行DFT计算得到Eads= -0.476eV,对应弱相互作用(图6d)。值得一提的是,该材料充分反...