prepared all figures, performed all measurements and took part in the analysis of the mechanism. I.A. took part in the analysis of the mechanism. C.R. was responsible for the coordination of the experiments and took part in the analysis of the mechanism. All authors reviewed the manuscript....
Sample holder: aluminum holder Test Example 5: Thermal Analysis The crystal obtained in Example 2 was accurately weighed into an aluminum sample pan and subjected to thermogravimetry (TG) and differential thermal analysis (DTA) under the following conditions. The results are shown in FIG. 5. (Mea...
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Most of the current studies on BoNT/HA have been based on genomic and amino acid sequence analysis. This approach has been proven erroneous in the case of a mosaic BoNT/DC, whose HC is very similar to BoNT/C based on sequence (~64% identity). However, the crystal structure of BoNT/DC...
First, using conditions in which the adduct at βThr220 should be predominant, the reaction was complete after 4 h at 25 ◦C, according to HPLC analysis (Figure S1A). The integrity of the protein after the treatment was further confirmed by the ability to assemble into microtubules (...
The molecular structures were solved by single-crystal X-ray crystal diffraction analysis. The complexes crystallized in the monoclinic crystal system in the P21/c (Ru1-2) and P21/n (Ru3) space groups. Density Functionals Theoretical (DFT) calculations were performed in methanol to gain an ...
3.1. X-Ray Crystallographic Analysis X-ray crystallographic data for compounds 4a, 7b, and 7d were collected from single crystals using an area detector diffractometer (Bruker AXS-KAPPA APEX II, Madison, WI, USA) at room temperature and graphite-monochromated Mo Kα (λ = 0.71073 Å) ...
After determination of the RVE size, such data can be used for damage evolution numerical analysis, which is conducted herein based on the CZM model applicable within the melt pool boundaries. By conducting sensitivity analyses, the CP material coefficients are calibrated based on uniaxial tensile ...
XPS Analysis of BYP:Ce3+ Crystal The survey scan report for the BYP:0.01Ce3+ crystal is shown in Figure 9a. The peaks observed in the XPS full spectrum have been found to be related to O, Y, Ba, P and Ce, which ensures the homogeneity of the sample at the atomic level without ...