The structure has been determined by single-crystal X-ray diffraction analysis (CIF files CCDC no. 1480230) and further characterized by elemental analyses, IR spectra, and thermogravimetric analysis. MOF I exhibits a rare (3,4)-connected 2D structure bearing two kinds of organic ligands. ...
CCDC 2043013: Experimental Crystal Structure DeterminationFurther information on research dataReferences (20) A.E. Thorarinsdottir et al. Chem. Rev. (2020)Y.J. Ma et al. J. Am. Chem. Soc. (2020) L.X. Sun et al. CrystEngComm (2010)H. Wang et al. Cryst. Growth Des. (2014)P. ...
(0.4mmol)HL和20mL去离子水的混合物在50℃下超声1h后密封在50mL聚四氟乙烯内衬的反应釜中,于140℃条件加热72h;(3)反应结束后,降温冷却至室温,得到无色块状透明晶体,即为羧酸钡[Ba(L)(HO)]MOF分子荧光传感器(CCDC号:1953727).本发明的有益效果是:1,制备方法简单易行,原子经济,节能环保;2,制得物对溶液中...