prazosine base is reacted with excess NH4Cl in a mixt. of 2-methoxyethanol, H2O and HOAc to form (I), which is isolated and dried. The prod. is refluxed in MeOH to form (Ia). MeOH, which is heated in vacuo to form (Ia).SCHICKANEDER HELMUTGRAFE INGOMARAHRENS KURT HENNING...
The reaction of Mn0 and HgCl2 with triphenylacetic acid in a mixture of 2-methoxyethanol and toluene afforded complex [Mn2IICl2(O2CCPh3)2(2-methoxyethanol)3] (1) in very good yield. Repeating the same reaction and replacing 2-methoxyethanol with THF forms the complex [Mn3IICl3.04(O2CCPh...