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3.8. Solvothermal Synthesis One-dimensional SiC was produced in an autoclave at 600 ◦C by a Mg-catalysed co- reduction of silicon-tetrachloride and 2-ethoxyethanol. Researchers tested the solvothermal preparation of 1D (nanorods, nanobelts, nanowires) and 2D SiC nanomaterials (nanosheets and ...