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For convenient handling, the brittle PAOF samples were glued to a glass substrate with BF-2 glue, and then fixed in a holder. FTIR spectra of PAOFs were registered with a Thermo Nicolet Nexus IR-spectrometer (Thermo Fisher Scientific Inc., Waltham, MA, USA) with a wave number range of ...
The temperature of the mixed solution was 85 °C and we chose three different times of immersion treatment: (I) 5 min; (II) 3 × 5 min and (III) 3 × 5 min + 72 h exposure of the so treated sample in humid atmosphere over a distillated water (in thermo-stated glass cell at ...