Preparative Method: by heating at reflux a mixture of 2-chloromethyl-4-nitrophenol and Phosphorus Oxychloride in the presence of a catalytic amount of KCl. 1 Purification: by distillation.doi:10.1002/047084289X.rc120Alan ArmstrongAmerican Cancer Society...
2-(Benzo[d]thiazol-2-yl) phenol (3) was treated with 4-nitrophenyl phosphorodichloridate(4) to obtain the monochloro intermediate, 2-(benzo[d]thiazol-2-yl)phenyl (4-nitrophenyl) phosphorochloridate(5). It was subsequently reacted with various amines, 6(a-j) to afford the desired ...
4-Nitrophenylphosphorodichloridate: CIL-CNLM-539-H-0.25GL-精氨酸:HCL (13C6, 99%; 15N4, 99%) CIL-CNLM-539-H-0.1GL-精氨酸:HCL (13C6, 99%; 15N4, 99%) CIL-CLM-2265-H-0.5GL-精氨酸:HCL (13C6, 99%) CIL-CLM-2265-H-0.25GL-精氨酸:HCL (13C6, 99%) ...