6. NMR Spectrum13C NMR : in CDCl3 1H NMR : 400 MHz in CDCl3 gas IR : CCl4 solution IR : liquid film SOLUTION (10% CCl4 FOR 3800-1340, 10% CS2 FOR 1340-430) Mass 7. Synthesis Route78-77-3Total: 43 Synthesis Route ...
Chemical NamePropane, 1-bromo-2-(bromodifluoromethyl)-1,1,2,3,3,3-hexafluoro- CAS No.89608-24-2 Molecular FormulaC4Br2F8 Molecular Weight359.838 LogP6.70 (Predicted) PubChemID71325182 Synonyms1,3-Dibromo-1,1,2,3,3-pentafluoro-2-(trifluoromethyl)propane; 1-Bromo-2-[bromo(difluoro)methy...
After reprecipitation from ace- tone solution with absolute ether, mp 156-167 ~ The purity of the compound was confirmed by the elemental analysis data and the NMR spectra. The second isomer, namely the hydrobromide of 1-bromo-2-amino-2-methylpropane, cannot be ob- tained by the above ...