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The precipitate was filtered off, dried, and added to the Et2O–H2O mixture (80 mL/80 mL). The copper(II) chelate was decomposed by stirring with Na2EDTA (0.05 mol) at r.t. (25 ◦C) for 1 h. Then, the organic layer was separated, dried over sodium sulfate, and distilled. ...
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