催化剂制备:对于 Bi:x%In/C(x = 0、5、10、15、20)(此处的 x % 代表初始进料中In和Bi的摩尔比),将 1.1764 g(4 mmol)C6H5Na3O7∙2H2O 加入装有 100 mL 去离子水的锥形瓶中,使其充分溶解和混合,然后加入指定摩尔比的 BiCl3 和 InCl3-4H2O。搅拌 0.5 小时后,向混合物中加入 0.05 克 XC-72...
SM3–SM7), H2O2and Cl2are used by adding a certain concentration for the elimination of ARBs and ARGs. They achieve elimination efficiencies between 70 and 100% in 10 to 30 min of treatment, with different efficiencies depending on the disinfectant...
Following this procedure, 2.5 g of zeolite 13X are dissolved in a 0.2 M copper-ammonia solution, which is formed by adding 15 mL of 28 vol% ammonium hydroxide (NH4OH) solution to 110 mL of 0.2 M Cu(NO3)2 ∙ 3H2O aqueous solution. The suspension is continuously stirred at room ...
Iron(III) nitrate nonahydrate (Fe(NO3)3∙9H2O, 200 mg), glucose (C6H12O6, 200 mg) and ammonium sulfate ((NH4)2SO4, 600 mg) were used as the precursors of iron, carbon and nitrogen, respectively. The precursors were mixed with 3 ml of Milli-Q water and ultrasonicated for 10 min....
以SrCO3、SrF2、Sc2O3和Mn(NO3)2∙6H2O为原料, 充分研磨后于1200 ℃下煅烧制得。如图7(a)所示, 在Sr2ScO3F中, Sc3+与5个O2-+1个F-形成ScO5F八面体[27];如图7(b)所示, Mn4+在Sr2ScO3F中表现出低光子能量发光且热猝灭现象严重。当Mn4+取代Sc3+时可能的电荷补偿机制是O2-取代F-而形成MnO6八面...
rac-1-[3-(3,6-Diphenyl-9-azatricyclo[4.3.1.03,7]decan-9-yl)propyl]piperidine-3-carboxylic acid rac-11d According to GP4: Ester rac-19d (19 mg, 39 µmol, 1.0 equiv) and Ba(OH)2 ∙ 8 H2O (49 mg, 0.16 mmol, 4 equiv). The product was obtained as colorless oil (15...
Sr2Fe1.5-xNixMo0.5O6-δ powders with the Ni doping content of 0, 0.1, 0.2, and 0.3 (SFMNix, x = 0, 0.1, 0.2, and 0.3) were synthesized by a glycine and citric acid assisted combustion method [19]. Stoichiometric amount of Sr(NO3)2, Fe(NO3)3•9H2O, (NH4)6Mo7O24∙4H2O ...
[N a2CO3] + 0.167 ⋅ [NaCl] − 1.3025) (2) where P, T, and I represent the pressure (MPa), temperature (°C), and the ionic strength of the solution system (M), respectively; [X] indicates the concentration of the solute X (M); v1 and ν1θ denote the ν1-CO32− ...
(1). All samples were prepared in D2O, whereas DNO3 and NaOD were used to adjust the pH. All solutions were prepared as 0.1 M NaGluc and let equilibrate for 3 days. Provided the very slow kinetics of the lactonization/hydrolysis reactions, the lactone 13C NMR peaks (both for γ-H...
The crystal structures of LiAl-X-mH2O (X = Cl−, NO3−, Br−) and of their dehydrates, LiAl-X, were determined by Besserguenev et al. [15]. In the dehydrates LiAl-X, Li and X form Li⋯⋯X⋯⋯Li⋯⋯X⋯⋯ chains along the c-axis, while the inter chain X⋯...